150 and More Basic NMR Experiments: A Practical CourseWiley, 10.09.1998 - 596 Seiten S. Braun, H.-O. Kalinowski, S. Berger 150 and More Basic NMR Experiments A Practical Course Explore the full productivity of your NMR equipment!
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The NMR Spectrometer | 1 |
Exp 2 | 12 |
12 | 34 |
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11 evolution 13C decoupler pulse 13C NMR 1H NMR spectrum 1H transmitter pulse Acquisition Time requirement adjust AMX-500 spectrometer antiphase Apply zero filling attenuation and 90 calculated carbon CH₂ CHCl3 Chem chemical shift Comments COSY coupling constants decoupler attenuation described in Experiment double quantum Equation ethyl crotonate Experiment 3.1 Fourier transformation frequency heteronuclear homonuclear HSQC INEPT instrument inverse Literature Magn method middle of 1H multiplets NMR Spectroscopy NMR spectrum 02 normal ¹H NMR note the offsets nuclei Observations Experiment parameters Phase correction Phase Cycle ¹H phase-sensitive points in F2 probe-head processing as described Processing Use standard proton pulse p2 pulse program Pulse Scheme pulsed field gradients quantum filter real data points Record a normal Reson Result The figure Scheme and Phase selective pulse shim signal spectra spectral width spin-lattice relaxation spin-spin coupling standard ID processing technique temperature transmitter attenuation transmitter pulse d1 δΗ