150 and More Basic NMR Experiments: A Practical CourseWiley, 10.09.1998 - 610 Seiten S. Braun, H.-O. Kalinowski, S. Berger 150 and More Basic NMR Experiments A Practical Course Explore the full productivity of your NMR equipment!
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Inhalt
The NMR Spectrometer | 1 |
Determination of the PulseDuration | 15 |
The 90 13C Decoupler Pulse with Inverse Configuration | 28 |
Urheberrecht | |
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11 evolution 13C decoupler pulse 1H NMR spectrum 1H transmitter pulse Acquisition Time requirement adjust AMX-500 spectrometer antiphase Apply zero filling attenuation and 90 calculated carbon CHCl3 Chem chemical shift Comments coupling constants d1 pl aq decoupler attenuation described in Experiment double quantum Equation ethyl crotonate Experiment 3.1 Fourier transformation frequency HSQC increment for 11 instrument inverse Literature Magn method middle of 1H NMR Spectroscopy NMR spectrum p1 normal 1H NMR note the offsets nuclei Observations Experiment parameters Phase correction Phase Cycle phase-sensitive points in F1 probe-head processing as described Processing Use standard proton pulse p2 pulse program Pulse Scheme pulsed field gradients quantum filter r.f. pulse ratio real data points Record a normal Reson Result The figure Scheme and Phase selective pulse shim spectra spectral width spectrometer spin-lattice relaxation standard ID processing technique transmitter attenuation transmitter pulse d1 δε δΗ

